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1H_NMR, 13CNMR スペクトル一覧　モノテルペン












1H NMR: δ 0.92-0.93 (6H, 0.92 (s), 0.92 (s)), 1.14 (3H, s), 1.40-1.84 (4H, 1.55 (ddd, J = 15.7, 8.1, 4.2 Hz), 1.48 (dddd, J = 13.1, 8.1, 4.8, 4.3 Hz), 1.65 (dddd, J = 13.1, 8.1, 4.2, 1.5 Hz), 1.76 (ddd, J = 15.7, 8.1, 4.3 Hz)), 2.23-2.44 (2H, 2.29 (dd, J = 17.9, 4.9 Hz), 2.38 (dd, J = 17.9, 1.4 Hz)), 2.52 (1H, ddt, J = 4.9, 4.8, 1.4 Hz).




δ (ppm)
9.3
19.5
19.5
27.2
30.3
43.2
43.3
46.8
57.7
219.1













1H NMR: δ 0.99-1.00 (6H, 1.00 (s), 1.00 (s)), 1.54-1.68 (5H, 1.56 (s), 1.62 (ddd, J = 13.3, 6.1, 5.9 Hz), 1.59 (ddd, J = 13.3, 1.8, 1.7 Hz)), 2.06 (1H, dddd, J = 6.1, 3.0, 2.6, 1.8 Hz), 2.14-2.30 (3H, 2.21 (ddd, J = 15.5, 8.8, 3.0 Hz), 2.21 (dd, J = 5.9, 1.7 Hz), 2.23 (ddd, J = 15.5, 8.9, 2.6 Hz)), 5.29 (1H, dd, J = 8.9, 8.8 Hz).




δ (ppm)
22.8
23.6
23.6
31.5
31.6
38.1
41
47.3
116.1
144.2













1H NMR: δ 1.56 (3H, s), 1.72 (3H, s), 2.14-2.48 (5H, 2.33 (ddd, J = 14.9, 8.7, 3.5 Hz), 2.41 (dddd, J = 10.2, 10.1, 3.5, 2.6 Hz), 2.38 (dd, J = 14.4, 10.2 Hz), 2.42 (dd, J = 14.4, 2.6 Hz), 2.23 (ddd, J = 14.9, 10.1, 9.6 Hz)), 4.86 (1H, d, J = 1.3 Hz), 4.94-4.96 (2H, 4.95 (d, J = 1.3 Hz), 4.95 (d, J = 1.3 Hz)), 5.22 (1H, d, J = 1.3 Hz), 5.37 (1H, dd, J = 9.6, 8.7 Hz).




δ (ppm)
20.6
20.7
29.9
32.0
38.3
110.0
112.6
126.0
142.2
145.6
148.1













1H NMR: δ 1.40-1.59 (7H, 1.52 (s), 1.50 (dddd, J = 13.4, 10.1, 10.0, 3.9 Hz), 1.56 (s)), 1.62-1.87 (2H, 1.68 (dddd, J = 13.4, 4.0, 2.1, 1.9 Hz), 1.80 (dddd, J = 10.1, 10.0, 3.9, 2.1 Hz)), 2.00-2.35 (4H, 2.29 (ddd, J = 15.0, 5.2, 3.9 Hz), 2.18 (ddd, J = 14.3, 3.9, 1.9 Hz), 2.12 (ddd, J = 14.3, 10.0, 4.0 Hz), 2.08 (ddd, J = 15.0, 10.0, 7.7 Hz)), 4.94-4.96 (2H, 4.95 (d, J = 1.3 Hz), 4.95 (d, J = 1.3 Hz)), 5.21 (1H, dd, J = 7.7, 5.2 Hz).




δ (ppm)
20.6
23.3
28.0
30.6
30.9
41.2
110.0
120.8
133.5
149.3












1H NMR: δ 1.54 (3H, s), 1.57-1.57 (6H, 1.57 (s), 1.57 (s)), 2.16 (2H, t, J = 7.4 Hz), 2.27 (2H, td, J = 7.4, 7.2 Hz), 5.22 (1H, t, J = 7.2 Hz), 6.20 (1H, s).




δ (ppm)
18.1
21.8
21.8
26.3
30.0
109.6
124.1
131.7
171.1













1H NMR: δ 1.39 (3H, s), 1.53-1.54 (6H, 1.54 (s), 1.54 (s)), 1.56-1.64 (2H, 1.60 (t, J = 7.4 Hz), 1.60 (t, J = 7.4 Hz)), 1.97-2.09 (2H, 2.03 (td, J = 7.4, 7.1 Hz), 2.03 (td, J = 7.4, 7.1 Hz)), 4.97-5.12 (2H, 5.02 (dd, J = 16.4, 1.4 Hz), 5.08 (dd, J = 10.9, 1.4 Hz)), 5.23 (1H, t, J = 7.1 Hz), 5.88 (1H, dd, J = 16.4, 10.9 Hz).




δ (ppm)
21.8
21.8
27.2
27.7
42.2
74.3
111.7
124.6
131.7
138.7












1H NMR: δ 1.57-1.58 (6H, 1.57 (s), 1.57 (s)), 2.20 (2H, td, J = 7.4, 7.2 Hz), 2.27 (2H, t, J = 7.4 Hz), 4.94 (1H, d, J = 1.3 Hz), 5.00 (1H, dd, J = 10.9, 1.7 Hz), 5.09 (1H, d, J = 1.3 Hz), 5.13-5.25 (2H, 5.18 (dd, J = 17.5, 1.7 Hz), 5.23 (t, J = 7.2 Hz)), 6.29 (1H, dd, J = 17.5, 10.9 Hz).




δ (ppm)
21.8
21.8
26.1
30.8
113.8
115.0
124.1
131.7
139.8
145.8